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Eun-Bin Kim 1 Article
Effects of Hydrogen Reduction in Microstructure, Mechanical and Thermoelectric Properties of Gas Atomized n-type Bi2Te2.7 Se0.3 Material
Pradip Rimal, Sang-Min Yoon, Eun-Bin Kim, Chul-Hee Lee, Soon-Jik Hong
J Powder Mater. 2016;23(2):126-131.   Published online April 1, 2016
DOI: https://doi.org/10.4150/KPMI.2016.23.2.126
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AbstractAbstract PDF

The recent rise in applications of thermoelectric materials has attracted interest in studies toward the fabrication of thermoelectric materials using mass production techniques. In this study, we successfully fabricate n-type Bi2Te2.7Se0.3 material by a combination of mass production powder metallurgy techniques, gas atomization, and spark plasma sintering. In addition, to examine the effects of hydrogen reduction in the microstructure, the thermoelectric and mechanical properties are measured and analyzed. Here, almost 60% of the oxygen content of the powder are eliminated after hydrogen reduction for 4 h at 360°C. Micrographs of the powder show that the reduced powder had a comparatively clean surface and larger grain sizes than unreduced powder. The density of the consolidated bulk using as-atomized powder and reduced atomized powder exceeds 99%. The thermoelectric power factor of the sample prepared by reduction of powder is 20% better than that of the sample prepared using unreduced powder.

Citations

Citations to this article as recorded by  
  • Enhancing thermoelectric performance of K-doped polycrystalline SnSe through band engineering tuning and hydrogen reduction
    Nan Xin, Yifei Li, Guihua Tang, Longyun Shen
    Journal of Alloys and Compounds.2022; 899: 163358.     CrossRef
  • The effect of powder pre-treatment on the mechanical and thermoelectric properties of spark plasma sintered N-type bismuth telluride
    Ahmed A. Abdelnabi, Vickram Lakhian, Joseph R. McDermid, James S. Cotton
    Journal of Alloys and Compounds.2021; 874: 159782.     CrossRef
  • Investigation of Spark Plasma Sintering Temperature on Microstructure and Thermoelectric Properties of p-type Bi-Sb-Te alloys
    Jin-Koo Han, Dong-won Shin, Babu Madavali, Soon-Jik Hong
    Journal of Korean Powder Metallurgy Institute.2017; 24(2): 115.     CrossRef
  • The Preparation and Growth Mechanism of the Recovered Bi2Te3 Particles with Respect to Surfactants
    Hyeongsub So, Eunpil Song, Yong-Ho Choa, Kun-Jae Lee
    Journal of Korean Powder Metallurgy Institute.2017; 24(2): 141.     CrossRef
  • Enhanced thermoelectric cooling properties of Bi2Te3−xSex alloys fabricated by combining casting, milling and spark plasma sintering
    Seung Tek Han, Pradip Rimal, Chul Hee Lee, Hyo-Seob Kim, Yongho Sohn, Soon-Jik Hong
    Intermetallics.2016; 78: 42.     CrossRef

Journal of Powder Materials : Journal of Powder Materials